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STUDY OF STRUCTURAL AND MECHANICAL PROPERTIES OF ZIRCONIUM DIOXIDE REINFORCED MAGNESIUM ALUMINATE CERAMICS

https://doi.org/10.55452/1998-6688-2025-22-1-286-297

Abstract

Improving the mechanical properties of technical ceramics is an urgent task of modern ceramic materials science. There is a need to improve the mechanical properties of refractories based on MgAl2O4 spinel, since this spinel is characterized by impeccable resistance to high-temperature corrosion. The work is devoted to studying the microstructure, phase composition and mechanical properties of MgAl2O4-ZrO2 ceramics. Experimental samples were synthesized by the solid-phase method from powder compacts. For a comprehensive study of the microstructure and phase composition, scanning electron microscopy and X-ray diffraction were used. The mechanical properties of the ceramic samples were studied by measuring the strength of tablets in biaxial bending. Reinforcement of magnesium aluminate with zirconium dioxide was carried out to improve the mechanical properties of composite ceramics. It was found that a change in the fraction of the press powder can affect the shrinkage, density and mechanical properties of MgAl2O4-ZrO2 ceramic samples.

About the Authors

D. B. Borgekov
L.N. Gumilyov Eurasian National University; Institute of Nuclear Physics of the Ministry of Energy of the Republic of Kazakhstan
Kazakhstan

 PhD 

Astana

Almaty



D. I. Shlimas
L.N. Gumilyov Eurasian National University; Institute of Nuclear Physics of the Ministry of Energy of the Republic of Kazakhstan
Kazakhstan

 PhD 

Astana

Almaty



R. I. Shakirzyanov
L.N. Gumilyov Eurasian National University
Kazakhstan

Cand.Phys.-Math.Sc. 

Astana



Yu. A. Garanin
L.N. Gumilyov Eurasian National University; Institute of Nuclear Physics of the Ministry of Energy of the Republic of Kazakhstan
Kazakhstan

Master 

Astana

Almaty



S. A. Maznykh
L.N. Gumilyov Eurasian National University
Kazakhstan

Astana



N. O. Volodina
L.N. Gumilyov Eurasian National University
Kazakhstan

Master 

Astana



A. L. Kozlovskiy
L.N. Gumilyov Eurasian National University; Institute of Nuclear Physics of the Ministry of Energy of the Republic of Kazakhstan
Kazakhstan

 PhD 

Astana

Almaty



M. V. Zdorovets
L.N. Gumilyov Eurasian National University; Institute of Nuclear Physics of the Ministry of Energy of the Republic of Kazakhstan
Kazakhstan

 Cand.Phys.-Math.Sc. 

Astana

Almaty



References

1. Cherkassova N.Ju., Veselov S.V., Dudina D.V. and Kuz’min R.I. (2023) Osnovy tehnicheskoj keramiki: uchebnoe posobie, Novosibirsk: NGTU, p 106. [In Russian]

2. Garshin A.P. (2024) Materialovedenie. Tehnicheskaja keramika v mashinostroenii: uchebnik dlja vuzov. 2-e izd., ispr. i dop., Moscow: Jurajt, p. 296. [In Russian]

3. Sadik C., El Amrani I.E., Albizane A. (2014) Recent advances in silica-alumina refractory: A review. Journal of Asian Ceramic Societies, vol. 2, no. 2, pp. 83–96.

4. Smith J.D., Fahrenholtz W.G. (2008) Refractory oxides. Ceramic and Glass Materials, p. 87.

5. Braulio M.A.L. et al. (2011) Spinel-containing alumina-based refractory castables. Ceramics International, vol. 37, no. 6, pp. 1705–1724.

6. El-Amir A.A.M. et al. (2021) MgAl2O4-reinforced c-ZrO2 ceramics prepared by spark plasma sintering. Journal of the Korean Ceramic Society, vol. 58, no. 5, pp. 574–582.

7. Fouad O.A. et al. (2023) Fabrication and characterization of macroporous alumina-nano tetragonal zirconia-nano spinel ceramic composites. Materials Chemistry and Physics, vol. 301, p. 127617.

8. Ganesh I., Ferreira J.M.F. (2009) Synthesis and characterization of MgAl2O4–ZrO2 composites. Ceramics international, vol. 35, no. 1, pp. 259–264.

9. Shakirzyanov R.I., Borgekov D.B., Garanin Y.A., Kozlovskiy A.L., Volodina N.O., Shlimas D.I., Zdorovets M.V. (2024) Study of the effect of synthesis temperature and thermal aging on structural, dielectric properties and phase composition in NiO/NiAl2O4 composite ceramics. Materials Research Express, vol. 11, no. 7, p. 075507.

10. Boch P. (2007) Ceramic Materials: Processes, Properties and Applications, ed. Nièpce J.-C.


Review

For citations:


Borgekov D.B., Shlimas D.I., Shakirzyanov R.I., Garanin Yu.A., Maznykh S.A., Volodina N.O., Kozlovskiy A.L., Zdorovets M.V. STUDY OF STRUCTURAL AND MECHANICAL PROPERTIES OF ZIRCONIUM DIOXIDE REINFORCED MAGNESIUM ALUMINATE CERAMICS. Herald of the Kazakh-British technical university. 2025;22(1):286-297. (In Russ.) https://doi.org/10.55452/1998-6688-2025-22-1-286-297

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ISSN 1998-6688 (Print)
ISSN 2959-8109 (Online)