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UWAVE-2000 as an effective equipment for the microwave аssistant synthesis of N, N-diethyl-2-(mesitylamino)-N-benzyl-oxoethanamonium chloride – a compound with plant growth regulating activity

https://doi.org/10.55452/1998-6688-2022-19-3-45-53

Abstract

The synthesis of N,N-Diethyl-2-(mesitiylamino)-N-benzyl-oxoethanamonium chloride was carried out by N-alkylation with traditional method and using microwave and ultrasonic activation. The synthesized ionіс compound is characterized by IR, NMR 1H and 13C methods, and its growth-stimulating activity has been tested on Zea Mays L. maize seeds. The synthesis of N,N-Diethyl-2-(mesitilamino)-N-benzyl-oxoethanamonium chloride using unconventional methods such as microwave and ultrasonic activation resulted in higher yields in a shorter period of time than traditional method. The highest yield (98%) was achieved by microwave activation of UWAVE-2000 in a very short time, while in the classical caseit was lower and the reaction time was twenty-four times longer. The synthesized ionic compound positively influenced the germination and growth energy of maize seeds. In samples treated with solution N,N-Diethyl-2-(mesitylamino)-N-benzyl-oxoethanaminium chloride of mould lesions was not so many, so, the treatment of maize seeds with trimecaine benzyl chloride not only stimulates the plant growth, but also prevent fungi mould formation.

About the Authors

S. Ye. Tursynbek
School of Chemical & Biochemical Engineering, Satbayev University
Kazakhstan

Tursynbek Saniya Erzhanovna, Scientific reasearcher

Satpayev st. 22, 050000, Almaty



Kh. S. Rafikova
School of Chemical & Biochemical Engineering, Satbayev University
Kazakhstan

Rafikova Khadichakhan Sabirzhanovna, Senior researcher

Satpayev st. 22, 050000, Almaty



A. O. Akimbek
School of Chemical & Biochemical Engineering, Satbayev University
Kazakhstan

Akimbek Arailym Utegenovna, Scientific reasearcher

Satpayev st. 22, 050000, Almaty



Ye. Kamshyger
School of Chemical & Biochemical Engineering, Satbayev University
Kazakhstan

Kamshyger Erasyl Sayatovich, Scientific reasearcher

Satpayev st. 22, 050000, Almaty



G. A. Jamalova
School of Chemical & Biochemical Engineering, Satbayev University
Kazakhstan

Jamalova Gulya Abaevna, Scientific reasearcher

Satpayev st. 22, 050000, Almaty



M. N. Naukanova
Science of Industrial and Natural Processes
France

Naukanova Madina Nurzhanovna, PhD student

Campus of Saint-Etienne 158, Saint-Etienne



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Review

For citations:


Tursynbek S.Ye., Rafikova Kh.S., Akimbek A.O., Kamshyger Ye., Jamalova G.A., Naukanova M.N. UWAVE-2000 as an effective equipment for the microwave аssistant synthesis of N, N-diethyl-2-(mesitylamino)-N-benzyl-oxoethanamonium chloride – a compound with plant growth regulating activity. Herald of the Kazakh-British Technical University. 2022;19(3):45-53. https://doi.org/10.55452/1998-6688-2022-19-3-45-53

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ISSN 1998-6688 (Print)
ISSN 2959-8109 (Online)