MANAGED SYNTHESIS OF A NANOSTRUCTURED TWO-DIMENSIONAL ATOMIC CRYSTAL OF BISMUTH SELENID
Abstract
The paper analyzes the literature of modern methods for producing nanosuspensions and the orderly growth of nanofilms. A new method for the controlled synthesis of a high-quality nanostructured two dimensional atomic crystal of bismuth selenide is discussed. Using the “gas-solid” growth mechanism, the influence of such factors as temperature, gas supply rate on the controlled growth of a nanostructured two-dimensional atomic crystal of bismuth selenide 8 pm in length and 5 nm thick on mica having a lattice similar to copper taken as a matrix was investigated. It is shown that the optimal conditions for conducting controlled synthesis of high-quality bismuth selenide are 4900, time 40 minutes, gas flow rate within 30 cm3/s ÷ 80 cm3/s. The structural characteristics of the obtained samples of bismuth selenide were studied by modern methods of atomic force microscopy (Bruker Atomic Force Microscope, AFM, USA), scanning electron microscopy (SEM, Hitachi S-4800, Japan), optical microscopy (Olimpus, DX-51, Japan), Raman spectroscopy (HORIBA LabRAM HR 800, USA), UV-VIS, transmission electron microscopy (TEM). The forms and properties of the synthesized samples of nanostructured atomic crystals of bismuth selenide are
About the Authors
М. EsjanulyKazakhstan
B. Bekturgankyzy
Kazakhstan
D. Kh. Kamysbayev
Kazakhstan
B. A. Serikbayev
Kazakhstan
A. K. Kokanbayev
Kazakhstan
L. K. Kudreyeva
Kazakhstan
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Review
For citations:
Esjanuly М., Bekturgankyzy B., Kamysbayev D.Kh., Serikbayev B.A., Kokanbayev A.K., Kudreyeva L.K. MANAGED SYNTHESIS OF A NANOSTRUCTURED TWO-DIMENSIONAL ATOMIC CRYSTAL OF BISMUTH SELENID. Herald of the Kazakh-British Technical University. 2019;16(4):54-62. (In Kazakh)