kaz29Вестник Казахстанско-Британского технического университетаHerald of the Kazakh-British Technical University1998-66882959-8109Казахстанско-Британский Технический Университетkaz29-203Research ArticleФИЗИКО-МАТЕМАТИЧЕСКИЕ И ТЕХНИЧЕСКИЕ НАУКИPHYSICAL, MATHEMATICAL AND TECHNICAL SCIENCESОПТИМИЗАЦИЯ ПРОЦЕССА ПЛАЗМО-ХИМИЧЕСКОГО СИНТЕЗА ФУЛЛЕРЕНОВOPTIMIZATION OF THE PLASMA-CHEMICAL SYNTHESIS PROCESS OF FULLERENESАхановаН. Е.AkhanovaN.

PhD-докторант

ГабдуллинМ. Т.GabdullinM.

первый проректор, к.ф.-м.н., PhD

ЩурД. В.SchurD.

СНС, к.х.н.

Казахстанско-Британский технический университетКазахстанИнститут проблем Материаловедения им. И.Н. ФранцевичаУкраина202009112021173119124Copyright © Аханова Н.Е., Габдуллин М.Т., Щур Д.В., 20212021Аханова Н.Е., Габдуллин М.Т., Щур Д.В.Akhanova N., Gabdullin M., Schur D.Данная работа распространяется под лицензией Creative Commons Attribution 4.0.This work is licensed under a Creative Commons Attribution 4.0 License.https://vestnik.kbtu.edu.kz/jour/article/view/203

Изучение особенностей синтеза фуллеренов даст возможность понимать процесс образования наноструктур этого класса. Увеличение выхода получения фуллеренов и чистота позволит приблизиться к созданию новых материалов экономичного класса. Данная работа посвящена экспериментальному методу получения фуллеренов методом дугового разряда. Установлено, что от параметров синтеза, в частности, давления газа, величин напряжения и силового тока, а также от подготовки электродов зависит чистота и выход фуллеренов. В данной работе показана десорбция графитовых электродов без использования вспомогательного оборудования. Для синтеза фуллеренов использован реактор, собранный по принципу Кретчмера, экстракция производилась раствором толуол.

Studying the features of the synthesis of fullerenes will make it possible to understand the process of formation of nanostructures of this class. Increasing the yield of fullerenes and purity will allow us to approach the creation of new materials of an economic class. This work is devoted to the experimental method for producing fullerenes by the arc discharge method. It was found that the purity and yield of fullerenes depend on the synthesis parameters, in particular the gas pressure, on the voltage, on the current strength, and also on the preparation of the electrodes. This paper shows the desorption of graphite electrodes without the use of auxiliary equipment. For the synthesis of fullerenes, a reactor assembled according to the Kretchmer principle was used, extraction was carried out with toluene solution. (Must be supplemented with at least 150 words should be)

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The authors declare that there are no conflicts of interest present.